CAPABILITIES
Secondary imaging can be carried out at short working distances with an overhead detector or at longer distances with a side-mounted detector and these SE detector signals can be isolated or mixed. Backscatter imaging can be accomplished at accelerating voltages as low as 1 kV at high resolution with the Hitachi-proprietary ExB detector. The menu based Windows software and greater automation will lead to greater ease of use for most individuals.
Energy dispersive analysis is provided via an ultra thin window detector. Analysis of elements from Boron through Uranium is possible with this detection system. It is interfaced with a Gresham Titan Analog HV Power Supply / Pulse Processor and 4Pi Spectral Engine Hardware with DTSA and Revolution Software. Software is available in these packages for X-ray mapping, qualitative, standardless and rigorous standards-based quantitative analysis.
About 4pi: 4pi Analysis, Inc. engineers and sells X-ray Microanalysis and Digital Imaging Systems. Logo used with permission. Disclaimer.
The S-4700 FE-SEM system is interfaced to the campus network so all user data can be downloaded to user storage systems from the laboratory.
TRAINING
eTraining
Free online eTraining is available for this instrument. This self-paced tutorial and reference content does not replace course requirements for authorized usage.
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Available topics related to this instrument:
Specimen Preparation Hitachi S-4700 FE-SEM |
Courses
Michigan Tech offers many undergraduate and graduate courses related to materials characterization.
One of these courses offers direct, hands-on training in field emission scanning electron microscopy:
MY 5200 - Advanced Scanning Electron Microscopy
Basic design and operating principles of scanning electron microscope (SEM) with discussions on interactions of electrons with solids and resulting signal production, for analysis of heterogeneous materials using X-ray microanalysis, and applications to surface science. Includes practical training on advanced operation of SEM and FE-SEM (FE=field emission)* instruments with an emphasis on the production of high resolution images and quantitative X-ray analysis of specimen composition based on real and virtual standards. (*if available)
Credits: 3.0 Lec-Rec-Lab: (2-0-3) Semesters Offered: Summer
Restrictions: Must be enrolled in one of the following Level(s): Graduate

Last updated February 3, 2010
Disclaimer
This is to notify you that the material you are accessing is not an official web page of Michigan Technological University, MCFF, or ACMAL. While MTU recognizes the constitutional right of free speech for its University users of the Internet and the World Wide Web, it is not responsible, and hereby disclaims all liability for any data, information, or opinions contained in unofficial web pages. Any comments related to the contents of personal home pages should be directed to the author of the pages. There is no affiliation between ACMAL and JEOL. There is no affiliation between ACMAL and 4pi.
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